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116998-62-0

CHEMBRDG-BB 4024087 synthesis

1synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere
2: tin(II) chloride dihdyrate / ethanol / 3 h / Reflux; Inert atmosphere

References:

Han, Young Taek;Kim, Kyeojin;Son, Dohyun;An, Hongchan;Kim, Hee;Lee, Jeeyeon;Park, Hyun-Ju;Lee, Jeewoo;Suh, Young-Ger [Bioorganic and Medicinal Chemistry,2015,vol. 23,# 3,p. 579 - 587]

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