Butyl levulinate synthesis
- Product Name:Butyl levulinate
- CAS Number:2052-15-5
- Molecular formula:C9H16O3
- Molecular Weight:172.22
64-18-6
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$22.12/250ML
123-76-2
473 suppliers
$5.00/25g
71-36-3
1044 suppliers
$14.00/25mL
592-84-7
159 suppliers
$14.00/25g
2052-15-5
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$9.00/100g
Yield:2052-15-5 99.8% ，592-84-7 84.2%
Reaction Conditions:
with calcium(II) chloride in water monomer at 100; for 2.5 h;Temperature;Reagent/catalyst;
Steps:
1.1-1.3; 2.1-2.3; 3.1-3.3; 4.1-4.3; 5.1-5.3; 6.1-6.3; 5.1-5.3 Example 6
(1) after the cellulose hydrolyzate is concentrated, the concentrated hydrolyzate of cellulose is obtained, Add CaCl 4.0 g and n-butanol 18.5 g to 30 g of cellulose concentrated hydrolyzate, 100 insulation reaction for 2.5h, of which, The composition of cellulose concentrated hydrolyzate is levulinic acid 5.9g, Formic acid 2.3g, water 21.4g and other biomass hydrolysis by-products 0.4g; (2) the reaction is completed, the temperature is lowered to 45 ° C, the sedimentation is layered, and the organic phase is separated, The mass of the organic phase is 26.2g; (3) organic phase obtains butyl levulinate and butyl formate respectively through distillation, The yield of butyl formate was 84.2 wt.%, The yield of butyl levulinate was 99.8 wt.%;
References:
CN114315554,2022,A Location in patent:Paragraph 0042-0045; 0047-0050; 0052-0055; 0057-0060; ...
123-76-2
473 suppliers
$5.00/25g
71-36-3
1044 suppliers
$14.00/25mL
2052-15-5
181 suppliers
$9.00/100g
6270-56-0
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$11.00/1g
71-36-3
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$14.00/25mL
2052-15-5
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$9.00/100g
98-00-0
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$23.00/50g
71-36-3
1044 suppliers
$14.00/25mL
2052-15-5
181 suppliers
$9.00/100g
98-00-0
470 suppliers
$23.00/50g
2052-15-5
181 suppliers
$9.00/100g