ChemicalBook CAS DataBase List Bis(2-ethylhexyl)amine

Bis(2-ethylhexyl)amine synthesis

5synthesis methods

Product Name:Bis(2-ethylhexyl)amine
CAS Number:106-20-7
Molecular formula:C16H35N
Molecular Weight:241.46

104-76-7 Synthesis

104-76-7
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$5.00/10g

104-75-6 Synthesis

104-75-6
212 suppliers
$14.00/25mL

106-20-7
257 suppliers
$6.00/25g

Yield:-

Reaction Conditions:

with chlorocyclopentadienylbis(triphenylphosphine)ruthenium(II);urea;diphenylphosphinopropane in diethylene glycol dimethyl ether at 160; for 12 h;Autoclave;Inert atmosphere;

Steps:

2.3. General catalytic procedure for amination
General procedure: The autoclave was charged with 1-hexylalcohol (2.5 mmol) and urea (2.5 mmol) in 1mLdiglyme. [(Cp)RuCl(dppe)] (3percent mol) as catalyst, diphenylphosphinopropane (dppp)(0.07 mmol) as supporting ligand and 0.04 g K2CO3 as base was added. The autoclavewas closed, flushed with argon for 5 min and then temperature was adjusted at160 °C. After 12 h, the autoclave was cooled to room temperature and the productswere analyzed by gas chromatography.

References:

Dindar, Sara;Nemati Kharat, Ali [Journal of Coordination Chemistry,2020]

FullText

104-75-6 Synthesis

104-75-6
212 suppliers
$14.00/25mL

106-20-7
257 suppliers
$6.00/25g

References