Benzoic acid, 2-chloro-4-fluoro-, ethyl ester synthesis
- Product Name:Benzoic acid, 2-chloro-4-fluoro-, ethyl ester
- CAS Number:167758-87-4
- Molecular formula:C9H8ClFO2
- Molecular Weight:202.61
451-46-7
287 suppliers
$5.00/5g
167758-87-4
41 suppliers
$16.00/5g
Yield:167758-87-4 61%
Reaction Conditions:
with N-chloro-succinimide;trifluorormethanesulfonic acid;palladium diacetate;N-fluoropyridinium triflate in 1,2-dichloro-ethane at 90; for 6 h;Sealed tube;regioselective reaction;
References:
Sun, Xiuyun;Shan, Gang;Sun, Yonghui;Rao, Yu [Angewandte Chemie - International Edition,2013,vol. 52,# 16,p. 4440 - 4444][Angew. Chem.,2013,vol. 125,# 16,p. 4536 - 4540,5] Location in patent:supporting information
64-17-5
724 suppliers
$10.00/50g
2252-51-9
386 suppliers
$7.00/5g
167758-87-4
41 suppliers
$16.00/5g
64-17-5
724 suppliers
$10.00/50g
21900-54-9
167 suppliers
$13.00/1g
167758-87-4
41 suppliers
$16.00/5g