Benzene-d5-methanol, α-phenyl-, (-)- (9CI) synthesis
- Product Name:Benzene-d5-methanol, α-phenyl-, (-)- (9CI)
- CAS Number:99398-35-3
- Molecular formula:C13H12O
- Molecular Weight:184.24
Yield:99398-35-3 77%
Reaction Conditions:
Stage #1: bromobenzene-d5with magnesium in tetrahydrofuran;ethylene dibromide at 0 - 60; for 0.75 h;
Stage #2: benzaldehyde in tetrahydrofuran;ethylene dibromide at 0; for 0.5 h;
References:
Mo, Fanyang;Trzepkowski, Louis J.;Dong, Guangbin [Angewandte Chemie - International Edition,2012,vol. 51,# 52,p. 13075 - 13079][Angew. Chem.,2012,vol. 124,# 52,p. 13252 - 13256,5] Location in patent:supporting information
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