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ChemicalBook CAS DataBase List ALPHA-(PHENYLTHIO)PHENYLACETIC ACID
10490-07-0

ALPHA-(PHENYLTHIO)PHENYLACETIC ACID synthesis

4synthesis methods
-

Yield:10490-07-0 70%

Reaction Conditions:

Stage #1: Benzyl phenyl sulfidewith n-butyllithium in tetrahydrofuran;hexane at 0; for 1 h;
Stage #2: carbon dioxide in tetrahydrofuran;diethyl ether;hexane;

References:

Baciocchi, Enrico;Giacco, Tiziana Del;Elisei, Fausto;Lapi, Andrea [Journal of Organic Chemistry,2006,vol. 71,# 3,p. 853 - 860]