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ChemicalBook CAS DataBase List ALLYL UNDECYLENATE
7493-76-7

ALLYL UNDECYLENATE synthesis

3synthesis methods
By azeotropic distillation of a benzene solution of the corresponding acid and allyl alcohol in the presence of naphthaleneβ-sulfonic acid.
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / neat (no solvent) / 24 h / 160 °C / Green chemistry
2: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / neat (no solvent) / 1 h / 140 °C / Microwave irradiation; Green chemistry

References:

Kreye, Oliver;Meier, Michael A. R. [RSC Advances,2015,vol. 5,# 65,p. 53155 - 53160]

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