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ChemicalBook CAS DataBase List ALLYL PHENYL SULFOXIDE
19093-37-9

ALLYL PHENYL SULFOXIDE synthesis

12synthesis methods
Oxidation of Allyl Phenyl Sulfide in dichloromethane with m-Chloroperbenzoic Acid acid (1.2 equiv) added slowly as a solution in dichloromethane at -70 °C affords the sulfoxide in high yields with minimal over-oxidation to the sulfone. The m-chlorobenzoic acid formed may be removed simply by filtration. Other oxidizing agents such as Sodium Bromite3 and Trifluoroperacetic Acid4 afford the sulfoxide in yields greater than 80% and are also highly selective.
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Yield:19093-37-9 100%

Reaction Conditions:

with 2-hydroperoxy-2-methoxypropane in methanol;

References:

Leriverend, Pierre;Leriverend, Marie-Louise [Synthesis,1987,# 6,p. 587 - 588]

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