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ChemicalBook CAS DataBase List ADENYLYL(3'>5')CYTIDINE FREE ACID
2382-66-3

ADENYLYL(3'>5')CYTIDINE FREE ACID synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) 2,4,6-collidine / 1.) THF, -78 deg C, 10 min, 2.) THF, -78 deg C, 15 min; 20 deg C, 30 min
2: 70 percent / 2 percent benzenesulfonic acid / CHCl3; methanol / 2 h / Ambient temperature
3: 1.) t-butylamine, 2.) methanolic ammonia, 3.) TBAF

References:

Ogilvie, Kelvin K.;Theriault, Nicole Y.;Seifert, Jan-Marcus;Pon, Richard T.;Nemer, Mona J. [Canadian Journal of Chemistry,1980,vol. 58,p. 2686 - 2693]

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