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ChemicalBook CAS DataBase List 7-Methyltryptamine
14490-05-2

7-Methyltryptamine synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1.1: tetrahydrofuran / 1 h / -40 °C / Inert atmosphere
2.1: trichlorophosphate / 1.5 h / Cooling with ice
2.2: 20 °C / Cooling with ice
2.3: 1 h / 105 °C
3.1: ammonium acetate / Reflux
4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

References:

Muratore, Michael E.;Shi, Lei;Pilling, Adam W.;Storer, R. Ian;Dixon, Darren J. [Chemical Communications,2012,vol. 48,# 51,p. 6351 - 6353]

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