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ChemicalBook CAS DataBase List 7-CHLORO-4-QUINAZOLINOL
31374-18-2

7-CHLORO-4-QUINAZOLINOL synthesis

11synthesis methods
-

Yield: 95%

Reaction Conditions:

in waterMicrowave irradiation;

Steps:

3.4.2
10g of compound BB1, formamidine acetate 8g (1.3eq) into 100ml eggplant-shaped flask, uniformly mixed, the microwave reaction 4πη (60% power). After cooling, 30ml of water was added, the solid was washed and filtered to give the BB2 compound 10g, yield 95%.

References:

SHANGHAIINSTITUTES FOR BIOLOGICAL SCIENCES, CAS;ShanghaiInstitute of Materia Medica (SIMM), Chinese Academy of Sciences (CAS),;WANG, HUI;LIU, HONG;LI, XIAOGUANG;ZHANG, XU;LIU, YANLING;GONG, NUOXI;CHEN, KERONG CN103570738, 2016, B Location in patent:Paragraph 0303; 0304; 0306

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