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ChemicalBook CAS DataBase List 6α-Noroxymorphol
58477-92-2

6α-Noroxymorphol synthesis

4synthesis methods
33522-95-1 Synthesis
7,8-Dihydro-14-hydroxy- normorphinone

33522-95-1
83 suppliers
$103.00/1mg

6α-Noroxymorphol

58477-92-2
3 suppliers
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Yield:58477-92-2 95%

Reaction Conditions:

with formic acid;triethylamine;[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2;N-[(1S,2S)-2-amino-1,2-diphenylethyl]-4-methylbenzenesulfonamide in acetonitrile at 20; for 24 h;

Steps:

8

Example 8: Epimeric Ratios and Yields[0082] Example 8 depicts the conversion of certain 6-keto morphinans (oxymorphone, noroxymorphone, oxycodone, naloxone, and naltrexone) to their corresponding 6-hydroxy morphinans. Specifically, the following table provides the epimeric ratio of 6-α-hydroxy morphinan to 6-β-hydroxy morphinan and the corresponding yields for each compound.

References:

WO2008/137672,2008,A1 Location in patent:Page/Page column 25