ChemicalBook CAS DataBase List 6-CHLORO-2-METHYLQUINOLINE

6-CHLORO-2-METHYLQUINOLINE synthesis

10synthesis methods

Product Name:6-CHLORO-2-METHYLQUINOLINE
CAS Number:92-46-6
Molecular formula:C10H8ClN
Molecular Weight:177.63

106-47-8 Synthesis

106-47-8
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$5.00/5 g

109-92-2 Synthesis

109-92-2
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$16.00/25mL

92-46-6
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$16.00/1g

Yield: 75%

Reaction Conditions:

with magnetite-palladium-graphene nanocomposite in acetonitrile at 80; for 12 h;

Steps:

Typical experimental procedure
General procedure: A 50 mL round-bottom flask equipped with acondenser and a Teflon-coated stirrer bar was charged with a solution ofaniline (1 mmol) in acetonitrile (5 mL) catalyst 1 (10 mol %) and vinyl ether(3 mmol) was added and the mixture was heated in air at 80 C for the time asmentioned in Table 1. The progress of the reaction was monitored by TLC. Thesolvent was removed under reduced pressure, and the products were isolatedby column chromatography on silica gel (hexane/ethyl acetate) to giveproduct. The structures of the products were confirmed by comparison withreported spectroscopic data.

References:

Verma, Sanny;Verma, Deepak;Jain, Suman L. [Tetrahedron Letters,2014,vol. 55,# 15,p. 2406 - 2409]

106-47-8 Synthesis

106-47-8
470 suppliers
$5.00/5 g