5-TERT-BUTYL-2-METHYL-BENZOXAZOLE synthesis
- Product Name:5-TERT-BUTYL-2-METHYL-BENZOXAZOLE
- CAS Number:40874-54-2
- Molecular formula:C12H15NO
- Molecular Weight:189.25
17791-62-7
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40874-54-2
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Yield:40874-54-2 96%
Reaction Conditions:
Stage #1: N-(5-(t-butyl)-2-hydroxyphenyl)acetamidewith trichlorophosphate in chloroform;Reflux;
Stage #2: with sodium hydroxide;lithium hydroxide monohydrate in chloroform; pH=8;Cooling with ice;
References:
Li, Ke-Lai;Du, Zong-Bo;Guo, Can-Cheng;Chen, Qing-Yun [Journal of Organic Chemistry,2009,vol. 74,# 9,p. 3286 - 3292] Location in patent:supporting information; experimental part
1199-46-8
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123-54-6
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40874-54-2
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14777-27-6
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1199-46-8
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40874-54-2
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79-16-3
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1199-46-8
265 suppliers
$9.00/10g
40874-54-2
31 suppliers
$45.00/50mg