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77747-69-4

5-Nitroisocoumarin synthesis

11synthesis methods
-

Yield:77747-69-4 67%

Reaction Conditions:

with 1,1-dimethoxyethane;N,N-dimethyl-formamide in N,N-dimethyl-formamide at 110 - 120; for 7 h;

References:

Matsui;Sugiura;Nakai;Iguchi;Shigeoka;Takada;Odagaki;Nagao;Ushio;Ohmoto;Iwamura;Yamazaki;Arai;Kawamura [Journal of Medicinal Chemistry,1992,vol. 35,# 18,p. 3307 - 3319]