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ChemicalBook CAS DataBase List 4-(HEXYLOXY)-4'-BIPHENYLCARBOXYLIC ACID
59748-16-2

4-(HEXYLOXY)-4'-BIPHENYLCARBOXYLIC ACID synthesis

6synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: 97 percent / sulfuric acid / 6 h / Heating
2.1: potassium carbonate / butan-2-one / Heating
2.2: aq. potassium hydroxide / ethanol; H2O / 0.5 h / Heating
2.3: aq. HCl / H2O / 3 h / Heating

References:

Tokushige;Mihara;Koide [Molecular Crystals and Liquid Crystals,2004,vol. 414,p. 27 - 38]

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