4'-HEXYL-4-BIPHENYLCARBONITRILE synthesis
- Product Name:4'-HEXYL-4-BIPHENYLCARBONITRILE
- CAS Number:41122-70-7
- Molecular formula:C19H21N
- Molecular Weight:263.38
92-52-4
397 suppliers
$9.00/5g
41122-70-7
109 suppliers
$17.00/100mg
Yield:-
Steps:
Multi-step reaction with 4 steps
1: AlCl3 / CH2Cl2 / 5 h / Ambient temperature
2: 1) hydrazine hydrate, 2) KOH / 1) diethylene glycol, 130 deg C, 1 h, 2) diethylene glycol, 130 deg C, 2 h, then 160 deg C, 3 h
3: 1) TiCl4, 2) hydroxylamine hydrochloride, pyridine / 1) CH2Cl2, 0 deg C, 30 min, 2) ethanol, reflux, 2 h
4: 74 percent / acetic anhydride / 2 h / Heating
References:
Ruolene, Yu. I.;Adomenas, P. V.;Sirutkaitis, R. A.;Denis, G. I. [Journal of Organic Chemistry USSR (English Translation),1984,vol. 20,p. 1187 - 1191][Zhurnal Organicheskoi Khimii,1984,vol. 20,# 6,p. 1305 - 1310]
544-92-3
254 suppliers
$9.00/1g
75056-89-2
0 suppliers
inquiry
41122-70-7
109 suppliers
$17.00/100mg
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
0 suppliers
inquiry
41122-70-7
109 suppliers
$17.00/100mg
59662-31-6
58 suppliers
$30.80/1g
41122-70-7
109 suppliers
$17.00/100mg
59662-26-9
26 suppliers
$90.00/500mg
41122-70-7
109 suppliers
$17.00/100mg