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ChemicalBook CAS DataBase List 4-Bromo-3-nitrobenzene-1,2-diamine
147021-89-4

4-Bromo-3-nitrobenzene-1,2-diamine synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 4 steps
1: SnCl2*H2O / ethyl acetate; ethanol / 0.58 h / 70 °C
2: aq. SeO2 / ethanol / 0.5 h / Heating
3: concd. H2SO4, concd. HNO3 / 1 h / 10 °C
4: concd. HCl, 48percent HI / 2 h / Ambient temperature

References:

Keana;Kher;Sui Xiong Cai;Dinsmore;Glenn;Guastella;Huang;Ilyin;Lu;Mouser;Woodward;Weber [Journal of Medicinal Chemistry,1995,vol. 38,# 22,p. 4367 - 4379]

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