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ChemicalBook CAS DataBase List 4-BROMO-2,5-DIMETHOXY-PHENOL
557757-32-1

4-BROMO-2,5-DIMETHOXY-PHENOL synthesis

4synthesis methods
31558-41-5 Synthesis
4-Bromo-2,5-dimethoxybenzaldehyde

31558-41-5
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$7.00/250mg

4-BROMO-2,5-DIMETHOXY-PHENOL

557757-32-1
27 suppliers
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Yield:557757-32-1 99%

Reaction Conditions:

Stage #1: 4-bromo-2,5-dimethoxybenzaldehydewith 3-chloro-benzenecarboperoxoic acid in dichloromethane at 25; for 4 h;Baeyer-Villiger oxidation;
Stage #2: with sodium hydroxide in methanol at 25; for 1 h;

References:

Tisdale, Eric J.;Kochman, David A.;Theodorakis, Emmanuel A. [Tetrahedron Letters,2003,vol. 44,# 16,p. 3281 - 3284]

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