4-BROMO-1-(TRIISOPROPYLSILYL)-1H-INDOLE synthesis
- Product Name:4-BROMO-1-(TRIISOPROPYLSILYL)-1H-INDOLE
- CAS Number:412048-44-3
- Molecular formula:C17H26BrNSi
- Molecular Weight:352.38
52488-36-5
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Yield:412048-44-3 96%
Reaction Conditions:
Stage #1: 4-bromo-1H-indolewith sodium hydride in tetrahydrofuran;mineral oil at 0 - 20; for 0.5 h;
Stage #2: triisopropylsilyl chloride in tetrahydrofuran;mineral oil at 0 - 20;
References:
Cambeiro, Xacobe C.;Ahlsten, Nanna;Larrosa, Igor [Journal of the American Chemical Society,2015,vol. 137,# 50,p. 15636 - 15639] Location in patent:supporting information