6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione synthesis
- Product Name:6-methoxy-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione
- CAS Number:3271-05-4
- Molecular formula:C14H11NO3
- Molecular Weight:241.24
![6-bromo-2-methyl-1H-benz[de]isoquinoline-1,3(2H)-dione](/CAS/GIF/4116-90-9.gif)
Yield:-
Reaction Conditions:
with copper(ll) sulfate pentahydrate in methanol;Reflux;
Steps:
2 Example 2
A mixture of 1 eq of compound 1 and 1 eq of sodium methoxide was stirred and refluxed in MeOH. CuSO 4 ?5H 2 O was added as a catalyst. Evaporating the reaction mixture in vacuo, To the residue was added 1 M HCl. Filtration and purification to obtain compound 2; The structural formula of the compound 2 is as follows:
References:
CN109970729,2019,A Location in patent:Paragraph 0029; 0030
![1H-Benz[de]isoquinoline-1,3(2H)-dione, 6-chloro-2-methyl-](/CAS/20210111/GIF/4118-33-6.gif)
![1H-Benz[de]isoquinoline-1,3(2H)-dione, 2-methyl-6-nitro-](/CAS/20210111/GIF/39061-36-4.gif)
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