3-METHYLPHENYLZINC IODIDE synthesis
- Product Name:3-METHYLPHENYLZINC IODIDE
- CAS Number:312693-24-6
- Molecular formula:C7H7IZn
- Molecular Weight:283.42
625-95-6
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312693-24-6
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Yield:-
Reaction Conditions:
Stage #1: zincwith chloro-trimethyl-silane;ethylene dibromide;lithium chloride in tetrahydrofuran at 20; for 0.0833333 h;Schlenk technique;Glovebox;
Stage #2: 3-Iodotoluene in tetrahydrofuran; for 24 h;Schlenk technique;Glovebox;Reflux;
References:
Basnet, Prakash;Kc, Shekhar;Dhungana, Roshan K.;Shrestha, Bijay;Boyle, Timothy J.;Giri, Ramesh [Journal of the American Chemical Society,2018,vol. 140,# 46,p. 15586 - 15590] Location in patent:supporting information