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ChemicalBook CAS DataBase List 3-METHYL-3-TRIMETHYLSILYLOXY-1-BUTYNE
17869-77-1

3-METHYL-3-TRIMETHYLSILYLOXY-1-BUTYNE synthesis

3synthesis methods
-

Yield: 98%

Reaction Conditions:

with saccharin in neat (no solvent) at 70; for 2 h;Product distribution;trimethylsilylation of acetylenic alcohols and glycols; solvent, reaction time and temperature, saccharine addition varied;

References:

Demina, Maria;Velikanov, Andrey;Medvedeva, Alevtina;Larina, Lyudmila;Voronkov, Mikhail [Journal of Organometallic Chemistry,1998,vol. 553,# 1-2,p. 129 - 133]

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