3-Furanboronic acid synthesis
- Product Name:3-Furanboronic acid
- CAS Number:55552-70-0
- Molecular formula:C4H5BO3
- Molecular Weight:111.89
22037-28-1
335 suppliers
$24.00/5g
55552-70-0
322 suppliers
$11.00/1g
Yield:55552-70-0 82%
Reaction Conditions:
Stage #1:3-bromofurane with n-butyllithium;Triisopropyl borate in tetrahydrofuran;hexane at -78 - -2; for 1 h;
Stage #2: with hydrogenchloride in tetrahydrofuran;hexane for 0.75 h;
References:
Beaulieu, Pierre L.;Gillard, James;Bykowski, Darren;Brochu, Christian;Dansereau, Nathalie;Duceppe, Jean-Simon;Hache, Bruno;Jakalian, Araz;Lagace, Lisette;LaPlante, Steven;McKercher, Ginette;Moreau, Elaine;Perreault, Stephane;Stammers, Timothy;Thauvette, Louise;Warrington, Jeff;Kukolj, George [Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,# 19,p. 4987 - 4993]
22037-28-1
335 suppliers
$24.00/5g
5419-55-6
377 suppliers
$12.00/5g
55552-70-0
322 suppliers
$11.00/1g
22037-28-1
335 suppliers
$24.00/5g
13675-18-8
160 suppliers
$6.00/1g
55552-70-0
322 suppliers
$11.00/1g