Yield:-

Reaction Conditions:

with water in isopropyl alcohol at 25; for 6 h;Temperature;

Steps:

1.1; 3.1; 5.1 1) Preparation of chloropropyltris (trimethylsiloxy) silane;
In a reaction flask equipped with a reflux condenser,8.47 g (0.04 mol) of chloropropyltrichlorosilane and 26.06 g (0.24 mol) of trimethylchlorosilane were added,Under stirring at room temperature 21.62g (0.36mol) isopropanol was slowly added for alcoholysis reaction,Then, 6.48 g (0.36 mol) of deionized water was added dropwise,Stirred at room temperature for 6h,Then cooled to room temperature,The organic layer was separated,Washed with deionized water until neutral,Add anhydrous Na2SO4 overnight,The distillation under reduced pressure gave chloropropyltris (trimethylsiloxy) silane.

References:

Zhejiang Sci-tech University;Chen, Tao;Wang, Xinying;Wang, Jiping CN106349274, 2017, A Location in patent:Paragraph 0019; 0020; 0027; 0047; 0048; 0065; 0066

FullText