ChemicalBook CAS DataBase List 3,5-DIMETHOXYBENZOYL CHLORIDE

3,5-DIMETHOXYBENZOYL CHLORIDE synthesis

9synthesis methods

Product Name:3,5-DIMETHOXYBENZOYL CHLORIDE
CAS Number:17213-57-9
Molecular formula:C9H9ClO3
Molecular Weight:200.62

1132-21-4 Synthesis

1132-21-4
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$10.00/5g

17213-57-9
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$7.00/1g

Yield: 100%

Reaction Conditions:

with thionyl chloride in tetrahydrofuran;N,N-dimethyl-formamide at 50; for 4 h;

Steps:

General procedure: Dimethylformamide (1 drop) and SOCl2 were added to a solution of the corresponding acid inTHF, and the reaction mixture was stirred at room temperature for 30 min. Then, the mixture was heated to 50°C and stirred at this temperature for 4 h. After the complete conversion of the starting acid, the solvent was evaporated, and the product was used without further purification.

References:

Kelbysheva;Telegina;Abramova;Strelkova;Ikonnikov;Rodionov;Ezernitskaya;Lokshin;Loim [Russian Chemical Bulletin,2015,vol. 64,# 11,p. 2646 - 2654][Izv. Akad. Nauk, Ser. Khim.,2015,vol. 64,# 11,p. 2646 - 2654,9]

60319-09-7 Synthesis