3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE synthesis
- Product Name:3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE
- CAS Number:13636-88-9
- Molecular formula:C11H12OS2
- Molecular Weight:224.34
75-15-0
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98-86-2
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74-88-4
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13636-88-9
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Yield:13636-88-9 87%
Reaction Conditions:
Stage #1: carbon disulfide;acetophenonewith sodium tertiary butoxide in toluene at 0; for 5 h;Inert atmosphere;
Stage #2: iodomethane in methanol;toluene; for 0.25 h;Reflux;
References:
Smyth, Lynette A.;Matthews, Thomas P.;Horton, Peter N.;Hursthouse, Michael B.;Collins, Ian [Tetrahedron,2010,vol. 66,# 15,p. 2843 - 2854] Location in patent:experimental part
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74-83-9
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98-86-2
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$9.00/5g
13636-88-9
25 suppliers
$106.00/50MG
98-86-2
769 suppliers
$9.00/5g
74-88-4
346 suppliers
$15.00/10g
13636-88-9
25 suppliers
$106.00/50MG
67-56-1
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20365-21-3
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13636-88-9
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$106.00/50MG
![2-[bis(methylsulfanyl)methylidene]-1-phenylbutane-1,3-dione](/CAS/20180529/GIF/29866-41-9.gif)
29866-41-9
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13636-88-9
25 suppliers
$106.00/50MG