ChemicalBook CAS DataBase List 3-(1H-imidazol-1-yl)propane-1,2-diol

3-(1H-imidazol-1-yl)propane-1,2-diol synthesis

3synthesis methods

Product Name:3-(1H-imidazol-1-yl)propane-1,2-diol
CAS Number:34793-28-7
Molecular formula:C6H10N2O2
Molecular Weight:142.16

288-32-4 Synthesis

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Yield:34793-28-7 88%

Reaction Conditions:

with 1,4-diaza-bicyclo[2.2.2]octane in 5,5-dimethyl-1,3-cyclohexadiene at 110; for 6 h;

Steps:

5 Example 5

118g of glycerol carbonate,68g imidazole, 186g xylene and 1g DABCO were put into the flask, heated to reflux at 110 ° C for 6 hours, and the upper layer solvent was separated while hot.Then vacuum distillation1- (2,3-dihydroxy) propylimidazole, yield 88%.

References:

CN110776464,2020,A Location in patent:Paragraph 0016

288-32-4 Synthesis

288-32-4
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$5.00/25g