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(3Z)-3-(6H-benzo[c][1]benzothiepin-11-ylidene)-N,N-dimethylpropan-1-amine
(3Z)-3-(6H-benzo[c][1]benzothiepin-11-ylidene)-N,N-dimethylpropan-1-amine synthesis
1synthesis methods
- Product Name:(3Z)-3-(6H-benzo[c][1]benzothiepin-11-ylidene)-N,N-dimethylpropan-1-amine
- CAS Number:25627-38-7
- Molecular formula:C19H21NS
- Molecular Weight:295.44
![[3-(Dimethylamino)propyl]triphenylphosphonium bromide hydrobromide](/CAS/GIF/27710-82-3.gif)
![Dibenzo[b,e]thiepin-11(6H)-one](/CAS/GIF/1531-77-7.gif)
Yield:25627-38-7 49%
Reaction Conditions:
with n-butyllithium in tetrahydrofuran;hexane; for 10 h;Ambient temperature;
References:
Polivka, Zdenek;Licha, Irena;Taufmann, Petr;Svatek, Emil;Holubek, Jiri;Protiva, Miroslav [Collection of Czechoslovak Chemical Communications,1987,vol. 52,# 6,p. 1566 - 1581]