2-NITROTHIOPHENOL synthesis
- Product Name:2-NITROTHIOPHENOL
- CAS Number:4875-10-9
- Molecular formula:C6H5NO2S
- Molecular Weight:155.17
88-75-5
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: 1,4-diaza-bicyclo[2.2.2]octane / 1-methyl-pyrrolidin-2-one / 50 °C
1.2: 2.5 h / 50 °C
2.1: N,N-dimethyl acetamide / 0.17 h / 200 °C / Sealed tube; Microwave irradiation
3.1: sodium hydroxide
References:
Moseley, Jonathan D.;Lenden, Philip;Lockwood, Mark;Ruda, Katinka;Sherlock, Jon-Paul;Thomson, Anthony D.;Gilday, John P. [Organic Process Research and Development,2008,vol. 12,# 1,p. 30 - 40]
1155-00-6
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88-73-3
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
