2-methyl-1-(5-methyl-2-thienyl)propan-1-one synthesis
- Product Name:2-methyl-1-(5-methyl-2-thienyl)propan-1-one
- CAS Number:94199-67-4
- Molecular formula:C9H12OS
- Molecular Weight:168.26
554-14-3
260 suppliers
$6.00/5g
79-30-1
369 suppliers
$10.00/10g
94199-67-4
10 suppliers
$45.00/50mg
Yield:94199-67-4 70%
Reaction Conditions:
Stage #1: isobutyryl chloridewith Aluminum Chloride in dichloromethane at 20; for 0.166667 h;Friedel-Crafts Acylation;
Stage #2: 2-Methylthiophene in dichloromethane at 50; for 3 h;Friedel-Crafts Acylation;
References:
Li, Xiaohan;Wood, Alex B.;Lee, Nicholas R.;Gallou, Fabrice;Lipshutz, Bruce H. [Green Chemistry,2022,vol. 24,# 12,p. 4909 - 4914] Location in patent:supporting information