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ChemicalBook CAS DataBase List 2-ETHYLCYCLOHEXANONE
4423-94-3

2-ETHYLCYCLOHEXANONE synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi / tetrahydrofuran; hexane / 20 °C
1.2: tetrahydrofuran; hexane / Heating
2.1: PCy3 / [Rh(C8H14)2Cl]2 / toluene / 1 h / 150 °C
2.2: HCl; H2O / toluene

References:

Jun;Lee;Lim [Journal of the American Chemical Society,2001,vol. 123,# 4,p. 751 - 752]

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