2-CHLORO-5-METHOXYBENZONITRILE synthesis
- Product Name:2-CHLORO-5-METHOXYBENZONITRILE
- CAS Number:127667-00-9
- Molecular formula:C8H6ClNO
- Molecular Weight:167.59
623-12-1
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: n-butyllithium / tetrahydrofuran / 2 h / -78 °C
1.2: -78 - 20 °C
2.1: hydroxylamine hydrochloride / ethanol / 4 h / Reflux
3.1: acetic anhydride; triethylamine / tetrahydrofuran
References:
Hunan Huateng Pharmaceutical Co., Ltd.;Bu Gonggaofamingren CN107400099, 2017, A
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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13719-61-4
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