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ChemicalBook CAS DataBase List 2,6-Diisopropylphenyl isocyanate
28178-42-9

2,6-Diisopropylphenyl isocyanate synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: pyridine / CH2Cl2 / 1 h / 0 °C
2: KOH / methanol / 15 °C
3: 77 percent / (NH4)2S2O8 / AgNO3, Cu(OAc)2 / CH2Cl2; H2O / 2 h / 40 °C

References:

Minisci, Francesco;Fontana, Francesca;Coppa, Fausta;Yan, Yong Ming [Journal of Organic Chemistry,1995,vol. 60,# 17,p. 5430 - 5433]

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