2,4-DINITRO-2'-METHYLDIPHENYLAMINE synthesis
4synthesis methods
- Product Name:2,4-DINITRO-2'-METHYLDIPHENYLAMINE
- CAS Number:964-75-0
- Molecular formula:C13H11N3O4
- Molecular Weight:273.24
Yield:-
Reaction Conditions:
Stage #1: o-toluidinewith n-butyllithium in tetrahydrofuran;hexane at -78 - -70;Inert atmosphere;
Stage #2: meta-dinitrobenzene in tetrahydrofuran;hexane at -78 - 20;Inert atmosphere;
References:
Gulevskaya, Anna V.;Tyaglivaya, Inna N.;Verbeeck, Stefan;Maes, Bert U.W.;Tkachuk, Anna V. [ARKIVOC,2011,vol. 2011,# 9,p. 238 - 251] Location in patent:experimental part