2,3-DICHLORO-6-METHYLQUINOXALINE synthesis

4synthesis methods

Product Name:2,3-DICHLORO-6-METHYLQUINOXALINE
CAS Number:39267-05-5
Molecular formula:C9H6Cl2N2
Molecular Weight:213.06

6309-61-1 Synthesis

1,4-DIHYDRO-6-METHYLQUINOXALINE-2,3-DIONE

6309-61-1
59 suppliers
$5.00/100mg

39267-05-5
93 suppliers
$19.00/250mg

Yield:39267-05-5 96%

Reaction Conditions:

with thionyl chloride;N,N-dimethyl-formamide for 1 h;Reflux;

Steps:

General procedure for the chlorination of dihydroxyquinoxalines in 1-chlorobutane

General procedure: N,N-Dimethylformamide (0.5 mg, 0.0673 mmol) was added dropwise to a slurry of 2,3-dihydroxyquinoxaline (2.0 g,12.3 mmol) and thionyl chloride (2.92 g, 24.6 mmol) in1-chlorobutane (20 mL). The mixture was refluxed for 1h.Then cooled to ambient temperature, the obtained needles were filtered, washed with ethyl ether, and dried.

References:

Bouanane, Zohra;Bounekhel, Mahmoud;Elkolli, Meriem;Takfaoui, Abdelilah [Revue Roumaine de Chimie,2017,vol. 62,# 12,p. 903 - 906]

6309-61-1 Synthesis

6309-61-1
59 suppliers
$5.00/100mg

39267-05-5
93 suppliers
$19.00/250mg

References