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ChemicalBook CAS DataBase List 2,2,6,6-Tetramethylpiperidine
768-66-1

2,2,6,6-Tetramethylpiperidine synthesis

7synthesis methods
Many routes for the synthesis of TMP have been reported. One method starts with a conjugate addition reaction of ammonia to phorone. The intermediate triacetone amine is then reduced in a Wolff-Kishner reaction.
Preparation of 2,2,6,6-Tetramethylpiperidine
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1) FClO3, BF3*(C2H5)2O / 1) hexane, 0 deg C
2: 1) FClO3, BF3*(C2H5)2O / 1) hexane, 0 deg C

References:

Vigalok, A. A.;Lukashina, S. G.;Petrova, G. G.;Vigalok, I. V.;Levin, Ya. A. [Journal of Organic Chemistry USSR (English Translation),1987,vol. 23,p. 440 - 445][Zhurnal Organicheskoi Khimii,1987,vol. 23,# 3,p. 489 - 494]

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