2,2',4,4'-TETRABROMODIPHENYL ETHER synthesis
- Product Name:2,2',4,4'-TETRABROMODIPHENYL ETHER
- CAS Number:5436-43-1
- Molecular formula:C12H6Br4O
- Molecular Weight:485.79
615-58-7
211 suppliers
$10.00/500mg
5436-43-1
87 suppliers
$94.00/100mg
Yield:5436-43-1 89%
Reaction Conditions:
for 0.2 h;Reagent/catalyst;
Steps:
1 Example 1Preparation of tetrabromobiphenyl ether-47
SiO2-Zr2 (0.05g) and 2,4-dibromophenol (2.50g) were mixed in a mortar and ground for 12 minutes,The product was separated by silica gel column chromatography using n-pentane as eluent to give 2.16 g of a white solid in 89% yield.
References:
Shandong Analysis Beta Center;Ji Wenhua;Zhao Rusong;Wang Xiao;Geng Yanling;Wang Xia CN106957218, 2017, A Location in patent:Paragraph 0043-0047
615-58-7
211 suppliers
$10.00/500mg
108-36-1
454 suppliers
$10.00/1g
5436-43-1
87 suppliers
$94.00/100mg
51452-87-0
17 suppliers
$499.27/5MG
5436-43-1
87 suppliers
$94.00/100mg
101-84-8
589 suppliers
$5.00/25g
5436-43-1
87 suppliers
$94.00/100mg