tert-butyl 6-oxo-2-azaspiro[4.4]nonane-2-carboxylate(WX101410) synthesis
- Product Name:tert-butyl 6-oxo-2-azaspiro[4.4]nonane-2-carboxylate(WX101410)
- CAS Number:1319716-43-2
- Molecular formula:C13H21NO3
- Molecular Weight:239.31
1319716-35-2
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1319716-43-2
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: Grubbs catalyst first generation / dichloromethane / 20 °C
2.1: tert.-butylhydroperoxide; palladium 10% on activated carbon; potassium carbonate / dichloromethane / 0 - 20 °C
3.1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate
4.1: dimethylsulfide borane complex / tetrahydrofuran / 40 °C
4.3: 0 - 20 °C / Molecular sieve
References:
Kang, Fu-An;Sui, Zhihua [Tetrahedron Letters,2011,vol. 52,# 32,p. 4204 - 4206]
![2-Azaspiro[4.4]non-7-ene-2-carboxylic acid, 1-oxo-, 1,1-dimethylethyl ester](/CAS/20210305/GIF/1319716-36-3.gif)
1319716-36-3
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1319716-43-2
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85909-08-6
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1319716-43-2
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