1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene synthesis
1synthesis methods
- Product Name:1-Bromo-4,4,5,5,6,6,6-heptafluoro-3,3-bis(trifluoromethyl)hex-1-ene
- CAS Number:128454-94-4
- Molecular formula:C8H2BrF13
- Molecular Weight:424.98
Yield:128454-94-4 90%
Reaction Conditions:
with tetrabutylammomium bromide in dichloromethane at 80; for 7 h;other nucleophiles possible (NaN3, NaNO2, KSCN, KCN), other solvents possible (C2H4Cl2, ethyl acetate);
References:
Rozhkov, I. N.;Igumnov, S. M.;Pletnev, S. I.;Chaplina, I. V. [Bulletin of the Academy of Sciences of the USSR Division of Chemical Science,1990,vol. 39,# 4.2,p. 856][Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya,1990,# 4,p. 951]