1,2-BENZENEDICARBONITRILE, 4-(2,2,3,3-TETRAFLUOROPROPOXY) synthesis
1synthesis methods
- Product Name:1,2-BENZENEDICARBONITRILE, 4-(2,2,3,3-TETRAFLUOROPROPOXY)
- CAS Number:121190-46-3
- Molecular formula:C11H6F4N2O
- Molecular Weight:258.17
Yield:121190-46-3 50%
Reaction Conditions:
Stage #1: 2,2,3,3-tetrafluoropropanol;4-Nitrophthalonitrile in dimethyl sulfoxide; for 0.166667 h;Inert atmosphere;
Stage #2: with potassium carbonate in dimethyl sulfoxide at 20;Inert atmosphere;
References:
Guerol, Ilke;Durmus, Mahmut;Ahsen, Vefa [European Journal of Inorganic Chemistry,2010,# 8,p. 1220 - 1230] Location in patent:experimental part