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ChemicalBook CAS DataBase List (1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE
27374-25-0

(1-ETHOXYCYCLOPROPOXY)TRIMETHYLSILANE synthesis

3synthesis methods
For the synthesis of the parent and the 2-monoalkyl-substituted compounds, reduction of ethyl 3- chloropropionate with sodium–potassium alloy in the presence of chlorotrimethylsilane in ether. A recent modification using ultrasound irradiation is much more convenient and more widely applicable. Other substituted derivatives are prepared by cyclopropanation of alkyl silyl ketene acetals with the Furukawa reagent (diiodomethane/diethylzinc).
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Yield:27374-25-0 75%

Reaction Conditions:

with zinc(II) iodide in diethyl ether for 48 h;Heating;

References:

Salauen, Jacques;Bennani, Fatima;Compain, Jean-Claude;Fadel, Antoine;Ollivier, Jean [Journal of Organic Chemistry,1980,vol. 45,# 21,p. 4129 - 4135]

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