1-Bromoadamantane synthesis
- Product Name:1-Bromoadamantane
- CAS Number:768-90-1
- Molecular formula:C10H15Br
- Molecular Weight:215.13
281-23-2
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$5.00/25g
768-90-1
407 suppliers
$10.00/5g
Yield:768-90-1 93%
Reaction Conditions:
with bromine at 85 - 110;Temperature;
Steps:
1 1-Bromodamantane preparation
In the reaction bottle,Add 30g of adamantane,Add 24 mL of liquid bromine to excess bromine.React at 85 ° C for 6 h,Then heat up to 110 ° C,Oil bath reaction for 3h,Place it overnight,Distillation of recovered bromine,The remaining bromine is reduced by using 20 mL of saturated sodium hydrogen sulfite solution.filter,The filter cake is washed to neutral,dry,Recrystallization of methanol,Light yellow crystal 44g,Yield 93%,That is 1-bromodamantane;
References:
Lanxi Aoerte Agricultural Technology Co., Ltd.;Guo Tingting CN109232270, 2019, A Location in patent:Paragraph 0026; 0028; 0037; 0046
768-95-6
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$10.00/5g
768-90-1
407 suppliers
$10.00/5g
935-56-8
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$34.50/5g
768-90-1
407 suppliers
$10.00/5g
828-51-3
422 suppliers
$10.00/5g
768-90-1
407 suppliers
$10.00/5g
