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ChemicalBook CAS DataBase List 1-Bromo-3,5-dimethoxybenzene
20469-65-2

1-Bromo-3,5-dimethoxybenzene synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 99 percent / thionyl chloride / dimethylformamide / 18 h / Heating
2: 60 percent / AIBN, CBrCl3, 2-mercaptopyridine N-oxide sodium salt / 0.25 h / Heating

References:

Dol, Georg C.;Kamer, Paul C. J.;Van Leeuwen, Piet W. N. M. [European Journal of Organic Chemistry,1998,# 2,p. 359 - 364]

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