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2101-89-5

1-AZIDO-3-BROMOBENZENE synthesis

4synthesis methods
-

Yield:2101-89-5 100%

Reaction Conditions:

Stage #1: 3-bromoanilinewith hydrogenchloride in water at 0;
Stage #2: with sodium nitrite in water at 0; for 0.333333 h;
Stage #3: with sodium azide in water at 0; for 3 h;

References:

Bertrand, Hélène C.;Schaap, Marjolein;Baird, Liam;Georgakopoulos, Nikolaos D.;Fowkes, Adrian;Thiollier, Clarisse;Kachi, Hiroko;Dinkova-Kostova, Albena T.;Wells, Geoff [Journal of Medicinal Chemistry,2015,vol. 58,# 18,p. 7186 - 7194] Location in patent:supporting information