1,2-BIS(PENTAMETHYLDISILOXANYL)ETHANE synthesis
4synthesis methods
- Product Name:1,2-BIS(PENTAMETHYLDISILOXANYL)ETHANE
- CAS Number:6231-68-1
- Molecular formula:C12H34O2Si4
- Molecular Weight:322.74
Yield:6231-68-1 93%
Reaction Conditions:
with C29H23Br2CoN2;trimethylsilylmethyllithium in toluene;pentane at 22; for 1 h;Inert atmosphere;
References:
Lee, Kangsang L. [Angewandte Chemie - International Edition,2017,vol. 56,# 13,p. 3665 - 3669][Angew. Chem.,2017,# 129,p. 3719 - 3723] Location in patent:supporting information