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[ CAS No. 96-45-7 ] {[proInfo.proName]}

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Chemical Structure| 96-45-7
Chemical Structure| 96-45-7
Structure of 96-45-7 * Storage: {[proInfo.prStorage]}

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Quality Control of [ 96-45-7 ]

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Product Details of [ 96-45-7 ]

CAS No. :96-45-7 MDL No. :MFCD00005276
Formula : C3H6N2S Boiling Point : -
Linear Structure Formula :- InChI Key :PDQAZBWRQCGBEV-UHFFFAOYSA-N
M.W : 102.16 Pubchem ID :2723650
Synonyms :
Chemical Name :Ethlenethiourea

Safety of [ 96-45-7 ]

Signal Word:Danger Class:N/A
Precautionary Statements:P501-P273-P272-P260-P270-P202-P201-P264-P280-P302+P352-P308+P313-P337+P313-P305+P351+P338-P362+P364-P333+P313-P301+P312+P330-P405 UN#:N/A
Hazard Statements:H302-H320-H360-H372-H317-H402 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 96-45-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 96-45-7 ]

[ 96-45-7 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 96-45-7 ]
  • [ 5467-57-2 ]
  • [ 80412-14-2 ]
  • 2
  • [ 96-45-7 ]
  • [ 5147-80-8 ]
  • C5H4N2S2*C4H8N2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
95% In N,N-dimethyl-formamide; at 120℃; for 3h; General procedure: A mixture of cyclic thiourea 4a-e (1 mmol) and di(methylsulfanyl)methylenemalononitrile 5a (0.170 g, 1 mmol) in DMF (3 mL) was stirred at 120 C. Upon completion (3 h monitored by TLC), the solvent was removed by rotary evaporator under vacuum. The afforded orange solid washed by ethyl acetate and dried to give 1.
  • 3
  • [ 96-45-7 ]
  • [ 1197159-91-3 ]
  • N-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-4, 5-dihydro-1H-imidazol-2-amine [ No CAS ]
YieldReaction ConditionsOperation in experiment
22% With mercury dichloride; In N,N-dimethyl-formamide; at 140℃; for 16h; A mixture of <strong>[1197159-91-3]4-(4,6-dimorpholino-1,3,5-triazin-2-yl)aniline</strong> (40 mg, 0.12 mmol), imidazolidine-2-thione (15 mg, 0.15 mmol0 and mercury(II) chloride (40 mg, 0.15 mmol) in 2 mL of DMF was stirred at 140 C. 16 hr. Then the reaction mixture was cooled to room temperature and filtered through Celite. The filtration was concentrated and purified by reverse phase chromatography to give N-[4-(4,6-dimorpholin-4-yl-1,3,5-triazin-2-yl)phenyl]-4, 5-dihydro-1H-imidazol-2-amine (9.0 mg, 22% yield). HPLC: Rt=1.74 min; MS 411 [M+H]
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