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[ CAS No. 938-18-1 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 938-18-1
Chemical Structure| 938-18-1
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Quality Control of [ 938-18-1 ]

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Product Citations

Product Details of [ 938-18-1 ]

CAS No. :938-18-1 MDL No. :MFCD00013650
Formula : C10H11ClO Boiling Point : -
Linear Structure Formula :(C6H2(CH3)3)C(O)Cl InChI Key :UKRQMDIFLKHCRO-UHFFFAOYSA-N
M.W : 182.65 Pubchem ID :97038
Synonyms :

Safety of [ 938-18-1 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3265
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 938-18-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 938-18-1 ]

[ 938-18-1 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 938-18-1 ]
  • [ 4761-00-6 ]
  • 2
  • [ 33893-89-9 ]
  • [ 938-18-1 ]
  • C38H31IrN5O(1+)*F6P(1-) [ No CAS ]
  • 3
  • [ 33893-89-9 ]
  • [ 938-18-1 ]
  • [ 1415251-75-0 ]
YieldReaction ConditionsOperation in experiment
84% With pyridine;Inert atmosphere; Reflux; The reaction was performed with 5-(2'-pyridyl)-1H-tetrazole (730 mg, 4.96 mmol) and 2,4,6-trimethylbenzoyl chloride (906 mg, 0.83 mL, 4.96 mmol, AlfaAesar) in pyridine (3.5 mL). The reaction mixture was diluted with water (50 mL) to give suspension. It was stirred for 10 min. The precipitate of the crude product was filtered, washed with water, and extracted with ether/H2O. The organic layer was washed with water and evaporated. Purification by column chromatography was performed on silica (15 g). Elution with CH2Cl2 removed pale yellow impurity. Elution with 0.5% CH3OH in CH2Cl2 recovered the product. White solid: 1.10 g (4.15 mmol, 84%). Anal. Calc. for C16H15N3O (MW 265.31): C, 72.43; H, 5.70; N, 15.84. Found: C, 72.24; H, 5.74; N, 15.53%. 1H NMR (400 MHz, [D6]dmso): delta = 8.79 (dd, J = 4.8, 0.8 Hz, 1H), 8.24 (dd, J = 8.0, 0.8 Hz, 1H), 8.12-8.04 (m, 1H), 7.69-7.62 (m, 1H), 7.09 (s, 2H), 2.33 (s, 3H), 2.25 (s, 6H) ppm. 13C NMR (100 MHz, CD2Cl2): delta = 164.96, 164.51, 150.52, 144.09, 141.48, 138.98, 137.39, 129.06, 125.98, 123.13, 121.19, 21.26, 20.44 ppm. GC-EI+ MS: m/z 265 (M+, 100%).
  • 4
  • C21H29OP [ No CAS ]
  • [ 938-18-1 ]
  • [ 1625-91-8 ]
  • 2,4,6-trimethylbenzoyl bis(4-tert-butylphenyl)phosphine oxide [ No CAS ]
  • 5
  • [ 30465-68-0 ]
  • [ 938-18-1 ]
  • 2-(5-methoxyquinolin-8-yl)-5,7-dimethylisoindolin-1-one [ No CAS ]
  • 6
  • [ 30465-68-0 ]
  • [ 938-18-1 ]
  • C20H20N2O2 [ No CAS ]
  • 7
  • [ 1593-60-8 ]
  • [ 938-18-1 ]
  • 4-methyl-N-((2,4,6-trimethylbenzoyl)oxy)benzenesulfonamide [ No CAS ]
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Technical Information

? Acyl Group Substitution ? Alkyl Halide Occurrence ? Baeyer-Villiger Oxidation ? Barbier Coupling Reaction ? Baylis-Hillman Reaction ? Benzylic Oxidation ? Birch Reduction ? Blanc Chloromethylation ? Bucherer-Bergs Reaction ? Catalytic Hydrogenation ? Clemmensen Reduction ? Complex Metal Hydride Reductions ? Corey-Bakshi-Shibata (CBS) Reduction ? Corey-Chaykovsky Reaction ? Fischer Indole Synthesis ? Friedel-Crafts Reaction ? General Reactivity ? Grignard Reaction ? Henry Nitroaldol Reaction ? Hiyama Cross-Coupling Reaction ? Horner-Wadsworth-Emmons Reaction ? Hydride Reductions ? Hydrogenolysis of Benzyl Ether ? Kinetics of Alkyl Halides ? Kumada Cross-Coupling Reaction ? Lawesson's Reagent ? Leuckart-Wallach Reaction ? McMurry Coupling ? Meerwein-Ponndorf-Verley Reduction ? Passerini Reaction ? Paternò-Büchi Reaction ? Petasis Reaction ? Peterson Olefination ? Pictet-Spengler Tetrahydroisoquinoline Synthesis ? Preparation of Aldehydes and Ketones ? Preparation of Alkylbenzene ? Preparation of Amines ? Prins Reaction ? Reactions of Aldehydes and Ketones ? Reactions of Alkyl Halides with Reducing Metals ? Reactions of Amines ? Reactions of Benzene and Substituted Benzenes ? Reformatsky Reaction ? Robinson Annulation ? Rosenmund Reduction ? Schlosser Modification of the Wittig Reaction ? Schmidt Reaction ? Specialized Acylation Reagents-Ketenes ? Stille Coupling ? Stobbe Condensation ? Substitution and Elimination Reactions of Alkyl Halides ? Suzuki Coupling ? Tebbe Olefination ? Ugi Reaction ? Vilsmeier-Haack Reaction ? Wittig Reaction ? Wolff-Kishner Reduction
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