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[ CAS No. 7378-99-6 ] {[proInfo.proName]}

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Chemical Structure| 7378-99-6
Chemical Structure| 7378-99-6
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Product Details of [ 7378-99-6 ]

CAS No. :7378-99-6 MDL No. :MFCD00009558
Formula : C10H23N Boiling Point : No data available
Linear Structure Formula :(CH3)2NC8H17 InChI Key :UQKAOOAFEFCDGT-UHFFFAOYSA-N
M.W : 157.30 Pubchem ID :16224
Synonyms :

Safety of [ 7378-99-6 ]

Signal Word:Danger Class:8,6.1
Precautionary Statements:P501-P270-P210-P264-P280-P370+P378-P303+P361+P353-P301+P330+P331-P363-P301+P310+P330-P304+P340+P310-P305+P351+P338+P310-P403+P235-P405 UN#:2922
Hazard Statements:H301-H314-H227 Packing Group:Ⅲ
GHS Pictogram:

Application In Synthesis of [ 7378-99-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7378-99-6 ]

[ 7378-99-6 ] Synthesis Path-Downstream   1~3

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YieldReaction ConditionsOperation in experiment
64%Chromat.; 23%Chromat. With platinum on carbon; sodium hydroxide; at 150℃; under 750.075 Torr; for 36h;Inert atmosphere; Autoclave; General procedure: After the reduction under a flow of H2 at 300C for 0.5h, we carried out catalytic tests without exposing the catalyst to air as follows. Methanol (30mmol) was injected to the reduced catalyst inside the glass tube through a septum inlet, thus the catalyst was covered with a layer of methanol to restrict it from air exposure. After removal of the septum under air, amine (1mmol), solid NaOH (1mmol), n-dodecane (0.25mmol) and a magnetic stirrer bar were placed in the tube. The tube was inserted into a stainless-steel autoclave (28cm3) and purged with N2 gas. Finally, the resulting mixture was heated at 150C and stirred under 1barN2. For the model reaction of n-octylamine, the catalyst screening, optimization of reaction conditions, kinetic studies and control reactions, the conversion of n-octylamine and yields of products were determined by GC analyses, using n-dodecane as an internal standard by applying the GC sensitivity of the isolated or commercial products. For the substrate scope study, the products were isolated by column chromatography with silica gel 60 (spherical, 60-100mum, Kanto Chemical Co., Ltd.) using hexane/ethyl acetate or ethyl acetate/methanol as the eluting solvent. The yields of the isolated amine derivatives were determined and identified by 1H and 13C NMR and GC-MS methods.
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