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[ CAS No. 7311-30-0 ] {[proInfo.proName]}

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Chemical Structure| 7311-30-0
Chemical Structure| 7311-30-0
Structure of 7311-30-0 * Storage: {[proInfo.prStorage]}

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Product Details of [ 7311-30-0 ]

CAS No. :7311-30-0 MDL No. :MFCD00026574
Formula : C13H29N Boiling Point : -
Linear Structure Formula :- InChI Key :OMEMQVZNTDHENJ-UHFFFAOYSA-N
M.W : 199.38 Pubchem ID :81746
Synonyms :

Safety of [ 7311-30-0 ]

Signal Word:Danger Class:8
Precautionary Statements:P264-P280-P301+P330+P331-P303+P361+P353-P304+P340+P310-P305+P351+P338+P310-P363-P405-P501 UN#:2735
Hazard Statements:H314 Packing Group:Ⅱ
GHS Pictogram:

Application In Synthesis of [ 7311-30-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7311-30-0 ]

[ 7311-30-0 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 7311-30-0 ]
  • [ 475-11-6 ]
  • (2S)-N-dodecyl-N,1-dimethylpyrrolidine-2-carboxamide [ No CAS ]
  • 2
  • [ 126-83-0 ]
  • [ 7311-30-0 ]
  • [ 1414933-00-8 ]
YieldReaction ConditionsOperation in experiment
91% With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 130℃; for 24h;Inert atmosphere; Sodium-3-chloro-2-hydroxy-1 -propanesulfonate (3.83 g, 19.5 mmol), N-methyldodecylamine (3 g, 15 mmol) and Nu,Nu-diisopropylethylamine (DIEA) (2.5 g, 19.5 mmol) are suspended in 20 mL of dry dimethylformamide (DMF) and heated to 130C under argon atmosphere for 24h. The volatiles are removed under reduced pressure and the residue is chromatographed on silica using dichloromethane/methanol using a stepwise increase of eluent strength from 9:1 to 4:1. Compound 1c is obtained as white material (4.61 g, 91 %).MS (ESI): 338.2 (M+H+), 675.5 (2M+H+), 697.5 (2M+Na+).1H-NMR (300 MHz, CDCI3): delta = 0.81 (t, J = 6.9, 3H), 1.1 -1.35 (m, 18H), 1.68 (m, 2H), 2.89 (d/d, J = 4.5/13.1 , 3H), 2.95-3.45 (m, 6H), 4.52 (m, 1 H), 8.90 (br. s, 1 H), 9.17 (br. s, 1 H).
  • 3
  • [ 7311-30-0 ]
  • [ 4263-52-9 ]
  • [ 2617-73-4 ]
YieldReaction ConditionsOperation in experiment
74% With potassium carbonate; In N,N-dimethyl-formamide; at 130℃;Inert atmosphere; Sodium-2-bromoethane sulfonate (41 1 mg, 1.95 mmol) and powdered K2C03 (269 mg, 1.95 mmol) are suspended in 3ml_ of dry DMF under argon atmosphere. N-methyldodecylamine (298 mg, 1.50 mmol) is added and the mixture stirred at 130C overnight. The volatiies are removed on a rotary evaporator and the residue purified by preparative HPLC and dried in high vacuum to yield 342 mg (74%) of 1q as a white solid.1H-NMR (300 MHz, CDCI3): delta = 0.81 (t, J = 6.4, 3H), 1.10-1.35 (m, 18H), 1 .70 (m, 2H), 2.88 (s), 2.89 (s,? = 3H), 3.0-3.45 (m, 5H), 3.55 (m, 1 H), 8.46 (br. s, 1 H), 8.89 (br. s, 1 H).MS (ESI): 308.2 (M+H+), 325.3 (M+NH4+), 615.4 (2M+H+).
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